Raman and X-ray investigations of LiFeSi2O6 pyroxene under pressure

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Raman and X-ray investigations of LiFeSi2O6 pyroxene under pressure

In situ Raman spectroscopy at high pressure was utilized to follow the phase transition of a synthetic sample of Li-aegerine pyroxene (LiFeSi2O6) from its low-pressure (C2/c) phase to its high-pressure (P21/c) phase. The phase change occurred between 0.7 and 1 GPa and was accompanied by a change in coordination of the Li atom from 4 to 5, which was confirmed by single-crystal X-ray diffraction....

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The first observation of the vibrational spectrum of the synthetic pyroxene Li-kosmochlor (LiCrSi2O6) is reported herein. The Raman and visible spectra are reported as a function of pressure. Though the pyroxene retains its P21/c symmetry, changes in the Raman spectra are observed between 6.8 and 7.7 GPa, possibly due to the formation of an additional bond between Li and O3 or some other transi...

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ژورنال

عنوان ژورنال: Journal of Raman Spectroscopy

سال: 2005

ISSN: 0377-0486,1097-4555

DOI: 10.1002/jrs.1373